Gas chromatographic and mass spectrometric identification of tetrachloroalkanoic and dichloroalkenoic acids in eel lipids

Research output: Contribution to journal › Journal article › Research › peer-review

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Gas chromatographic and mass spectrometric identification of tetrachloroalkanoic and dichloroalkenoic acids in eel lipids. / Mu, Huiling; Wesén, C.; Sundin, P.; Nilsson, E.

In: Journal of Mass Spectrometry, Vol. 31, No. 5, 01.05.1996, p. 517-526.

Research output: Contribution to journal › Journal article › Research › peer-review

Harvard

Mu, H, Wesén, C, Sundin, P & Nilsson, E 1996, 'Gas chromatographic and mass spectrometric identification of tetrachloroalkanoic and dichloroalkenoic acids in eel lipids', Journal of Mass Spectrometry, vol. 31, no. 5, pp. 517-526. https://doi.org/10.1002/(SICI)1096-9888(199605)31:5<517::AID-JMS325>3.0.CO;2-A

APA

Mu, H., Wesén, C., Sundin, P., & Nilsson, E. (1996). Gas chromatographic and mass spectrometric identification of tetrachloroalkanoic and dichloroalkenoic acids in eel lipids. Journal of Mass Spectrometry, 31(5), 517-526. https://doi.org/10.1002/(SICI)1096-9888(199605)31:5<517::AID-JMS325>3.0.CO;2-A

Vancouver

Mu H, Wesén C, Sundin P, Nilsson E. Gas chromatographic and mass spectrometric identification of tetrachloroalkanoic and dichloroalkenoic acids in eel lipids. Journal of Mass Spectrometry. 1996 May 1;31(5):517-526. https://doi.org/10.1002/(SICI)1096-9888(199605)31:5<517::AID-JMS325>3.0.CO;2-A

Author

Mu, Huiling ; Wesén, C. ; Sundin, P. ; Nilsson, E. / Gas chromatographic and mass spectrometric identification of tetrachloroalkanoic and dichloroalkenoic acids in eel lipids. In: Journal of Mass Spectrometry. 1996 ; Vol. 31, No. 5. pp. 517-526.

Bibtex

@article{9a9cb376261a46e898e5aa05be17f116,
title = "Gas chromatographic and mass spectrometric identification of tetrachloroalkanoic and dichloroalkenoic acids in eel lipids",
abstract = "Chlorinated fatty acid methyl esters, transesterified from the lipids of eel (Anguilla anguilla, obtained from the receiving waters of a chlorine bleaching pulp mill), were studied by gas chromatography (GC) using electrolytic conductivity detection and mass spectrometry (MS) with electron impact and ammonia positive-ion chemical ionization. GC retention indices and column difference values in combination with GC/MS demonstrated the presence of isomers of methyl dichlorotetradecenoate, methyl dichlorohexadecenoate, methyl dichlorooctadecenoate and methyl tetrachlorotetradecanoate. Isomers of methyl threo, threo-tetrachlorooctadecanoate were identified by co-injection of the eel sample and synthesized reference compounds. The results were confirmed by ammonia positive-ion chemical ionization high-resolution selective-ion monitoring of the ammonium adduct molecular ions.",
author = "Huiling Mu and C. Wes{\'e}n and P. Sundin and E. Nilsson",
year = "1996",
month = may,
day = "1",
doi = "10.1002/(SICI)1096-9888(199605)31:5<517::AID-JMS325>3.0.CO;2-A",
language = "English",
volume = "31",
pages = "517--526",
journal = "Journal of Mass Spectrometry",
issn = "1076-5174",
publisher = "JohnWiley & Sons Ltd",
number = "5",

}

RIS

TY - JOUR

T1 - Gas chromatographic and mass spectrometric identification of tetrachloroalkanoic and dichloroalkenoic acids in eel lipids

AU - Mu, Huiling

AU - Wesén, C.

AU - Sundin, P.

AU - Nilsson, E.

PY - 1996/5/1

Y1 - 1996/5/1

N2 - Chlorinated fatty acid methyl esters, transesterified from the lipids of eel (Anguilla anguilla, obtained from the receiving waters of a chlorine bleaching pulp mill), were studied by gas chromatography (GC) using electrolytic conductivity detection and mass spectrometry (MS) with electron impact and ammonia positive-ion chemical ionization. GC retention indices and column difference values in combination with GC/MS demonstrated the presence of isomers of methyl dichlorotetradecenoate, methyl dichlorohexadecenoate, methyl dichlorooctadecenoate and methyl tetrachlorotetradecanoate. Isomers of methyl threo, threo-tetrachlorooctadecanoate were identified by co-injection of the eel sample and synthesized reference compounds. The results were confirmed by ammonia positive-ion chemical ionization high-resolution selective-ion monitoring of the ammonium adduct molecular ions.

AB - Chlorinated fatty acid methyl esters, transesterified from the lipids of eel (Anguilla anguilla, obtained from the receiving waters of a chlorine bleaching pulp mill), were studied by gas chromatography (GC) using electrolytic conductivity detection and mass spectrometry (MS) with electron impact and ammonia positive-ion chemical ionization. GC retention indices and column difference values in combination with GC/MS demonstrated the presence of isomers of methyl dichlorotetradecenoate, methyl dichlorohexadecenoate, methyl dichlorooctadecenoate and methyl tetrachlorotetradecanoate. Isomers of methyl threo, threo-tetrachlorooctadecanoate were identified by co-injection of the eel sample and synthesized reference compounds. The results were confirmed by ammonia positive-ion chemical ionization high-resolution selective-ion monitoring of the ammonium adduct molecular ions.

UR - http://www.scopus.com/inward/record.url?scp=0029868196&partnerID=8YFLogxK

U2 - 10.1002/(SICI)1096-9888(199605)31:5<517::AID-JMS325>3.0.CO;2-A

DO - 10.1002/(SICI)1096-9888(199605)31:5<517::AID-JMS325>3.0.CO;2-A

M3 - Journal article

AN - SCOPUS:0029868196

VL - 31

SP - 517

EP - 526

JO - Journal of Mass Spectrometry

JF - Journal of Mass Spectrometry

SN - 1076-5174

IS - 5

ER -

ID: 102760708